Determination of Residual Acetamiprid and Imidacloprid in Unpolished Rice by Centrifugal Spin Column Clean-up and Water Mobile Phase HPLC-Diode Array

Furusawa, Naoto (2021) Determination of Residual Acetamiprid and Imidacloprid in Unpolished Rice by Centrifugal Spin Column Clean-up and Water Mobile Phase HPLC-Diode Array. In: New Innovations in Chemistry and Biochemistry Vol. 6. B P International, pp. 81-88. ISBN 978-93-5547-143-7

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Official URL: https://doi.org/10.9734/bpi/nicb/v6/2230C

Abstract

This chapter introduces a suitable analysis method for routine residual monitoring of antimicrobial drugs in food. A rapid, simple, and space-saving technique of sample preparation followed by a 100% water mobile phase high-performance liquid chromatography (HPLC) coupled photo-diode array detector (PDA) for quantifying acetamiprid (ATP) and imidacloprid (ICP) in unpolished rice was described here. The analytes were extracted from the sample using a handheld ultrasonic homogenizer with water, and purified by MonoSpin® C18-CX, a centrifugal monolithic silica spin mini-column, and quantified within 20 min sample-1. The accuracy, precision, and system suitability are well within the international method acceptance criteria.

Item Type:	Book Section
Subjects:	Asian STM > Chemical Science
Depositing User:	Managing Editor
Date Deposited:	16 Oct 2023 03:56
Last Modified:	16 Oct 2023 03:56
URI:	http://journal.send2sub.com/id/eprint/2299

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